Solid Phase Extraction

Solid Phase Extraction

Written by world-renowned experts in the field, the book contains helpful reference charts, tables of solvent properties, selectivities, molecular acid/base properties, and more.

Author: Nigel J.K. Simpson

Publisher: CRC Press

ISBN: 1420056247

Category: Science

Page: 528

View: 636

Demonstrating the relationship of the basic theory of solid-phase extraction (SPE) to chromatography, this comprehensive reference illustrates how SPE techniques significantly contribute to the preparation of samples for a wide variety of analytical techniques. It provides step-by-step details on the applications of SPE to environmental matrices, broad-spectrum drug screening, veterinary drug abuse, pharmaceutical drug development, biological samples, and high-throughput screening. Written by world-renowned experts in the field, the book contains helpful reference charts, tables of solvent properties, selectivities, molecular acid/base properties, and more.
Categories: Science

Solid Phase Extraction

Solid Phase Extraction

Written by world-renowned experts in the field, the book contains helpful reference charts, tables of solvent properties, selectivities, molecular acid/base properties, and more.

Author: Nigel J.K. Simpson

Publisher: CRC Press

ISBN: 082470021X

Category: Science

Page: 528

View: 203

Demonstrating the relationship of the basic theory of solid-phase extraction (SPE) to chromatography, this comprehensive reference illustrates how SPE techniques significantly contribute to the preparation of samples for a wide variety of analytical techniques. It provides step-by-step details on the applications of SPE to environmental matrices, broad-spectrum drug screening, veterinary drug abuse, pharmaceutical drug development, biological samples, and high-throughput screening. Written by world-renowned experts in the field, the book contains helpful reference charts, tables of solvent properties, selectivities, molecular acid/base properties, and more.
Categories: Science

Solid Phase Extraction

Solid Phase Extraction

The final section of the book discusses the latest SPE technology, with detailed coverage of the automation process, solid-phase extraction disks, and innovations such as solid-phase microextraction and small-volume solid-phase extraction.

Author: E. Michael Thurman

Publisher: Wiley-Interscience

ISBN: UCAL:B4378725

Category: Science

Page: 344

View: 953

Solid-Phase Extraction (SPE) offers accessible, up-to-date coverage of every aspect of this tremendously useful separation tool, from how it works and where it works to recent advances in equipment and techniques. Divided into three main parts, the book begins with a clear explanation of basic SPE concepts—including theory, chemistry, and mechanisms of interaction as well as methods development, troubleshooting, and optimization. The next section presents an in-depth look at SPE applications, with separate chapters devoted to clinical, environmental, and natural product chemistry. Numerous examples drawn from each of these three areas illustrate SPE in action in the real world, successfully bridging the gap between principles and practice. The final section of the book discusses the latest SPE technology, with detailed coverage of the automation process, solid-phase extraction disks, and innovations such as solid-phase microextraction and small-volume solid-phase extraction. Suggested reading and references are included throughout, providing a useful springboard for further research and study. Whether you are new to SPE or are looking to keep abreast of the newest developments in SPE methods and uses, Solid-Phase Extraction gives you instant access to the information you need—an essential companion for chemists of all types who use SPE in their work. Complete coverage of SPE concepts and applications—at your fingertips Solid-Phase Extraction (SPE) equips chemists in any field with an incomparable one-stop source of up-to-date information on SPE. With sections devoted to fundamental principles, applications, and new technology, it is both comprehensive and easy to use—the ideal working reference on this important subject. Presents a straightforward examination of SPE theory, methods development, chemistry, and mechanisms of interaction Provides detailed coverage of SPE applications in clinical, environmental, and natural product chemistry Features practical examples illustrating a range of real-world SPE uses Prepares chemists to make informed decisions on sorbent selection Covers the latest SPE technology, with valuable insights on automation and new sample preparation methods Offers suggestions for further reading, Internet resources, and product guides
Categories: Science

Forensic and Clinical Applications of Solid Phase Extraction

Forensic and Clinical Applications of Solid Phase Extraction

In Forensic and Clinical Applications of Solid Phase Extraction, hands-on experts explain the principles behind SPE and provide a host of readily reproducible protocols designed to allow the reader to master his or her extraction challenges ...

Author: Michael J. Telepchak

Publisher: Springer Science & Business Media

ISBN: 9781592592920

Category: Medical

Page: 370

View: 744

This complete laboratory reference manual explains the principles behind solid phase extraction (SPE) and provides readily reproducible protocols for solving extraction problems in forensic and clinical chemistry. Numerous actual chromatograms, based on original research and diverse applications, demonstrate the technique and the results that can be achieved. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and on avoiding known pitfalls.
Categories: Medical

Analytical Solid Phase Extraction

Analytical Solid Phase Extraction

This book describes what analytical scientists and technicians need to know about this emerging procedure: how it works, how to choose from available techniques, how to utilize it effectively in the laboratory.

Author: James S. Fritz

Publisher: Wiley-VCH

ISBN: UOM:39015047451466

Category: Science

Page: 209

View: 169

New trends in solid-phase extraction for analytical use--a practical introduction. Owing to its low cost, ease of use, and nonpolluting means of preparing samples for analysis, solid-phase extraction (SPE) is fast overtaking traditional liquid--liquid methods in clinical, pharmaceutical, agricultural, and industrial applications. This book describes what analytical scientists and technicians need to know about this emerging procedure: how it works, how to choose from available techniques, how to utilize it effectively in the laboratory. Along with the historical perspective and fundamental principles, this practical book reviews the latest literature on solid-phase materials, equipment, and applications--including EPA-endorsed techniques. Special features include: * Coverage of separation and uptake methods. * Promising developments in the use of membrane disks. * The advantages of using polymeric resins over silica materials. * Mechanism and use of ion-exchange materials for SPE. * A remarkably complete chapter on the extraction of metal ions. * Groundbreaking research in the miniaturized SPE technique. Readers seeking additional information on SPE procedures may wish to consult: SOLID-PHASE EXTRACTION, Principles and Practice, E. M. Thurman and M. S. Mills 1998 (0-471-61422-X) 384 pp. SOLID-PHASE MICROEXTRACTION Theory and Practice Janusz Pawliszyn 1997 (0-471-19034-9) 264 pp.
Categories: Science

Forensics and Clinical Applications of Solid Phase Extraction

Forensics and Clinical Applications of Solid Phase Extraction

This volume explains the principles behind SPE and provides protocols to help readers master extraction problems.

Author: Thomas F. August

Publisher: CRC Press

ISBN: 1466510951

Category: Law

Page: 420

View: 925

Solid Phase Extraction (SPE) has become a powerful and extensively used technique in the clean-up and concentration of samples in a wide variety of analytical techniques. This volume explains the principles behind SPE and provides protocols to help readers master extraction problems.
Categories: Law

Sample Preparation Techniques in Analytical Chemistry

Sample Preparation Techniques in Analytical Chemistry

Varian Sample Preparation Products, Inc., product literature, 2002. www.varianinc.com N. J. K. Simpson, Ion exchange extraction, in N. J. K. Simpson, ed., SolidPhase Extraction: Principles, Techniques, and Applications, Marcel Dekker, ...

Author: Somenath Mitra

Publisher: John Wiley & Sons

ISBN: 9780471457824

Category: Science

Page: 488

View: 696

The importance of accurate sample preparation techniques cannot be overstated--meticulous sample preparation is essential. Often overlooked, it is the midway point where the analytes from the sample matrix are transformed so they are suitable for analysis. Even the best analytical techniques cannot rectify problems generated by sloppy sample pretreatment. Devoted entirely to teaching and reinforcing these necessary pretreatment steps, Sample Preparation Techniques in Analytical Chemistry addresses diverse aspects of this important measurement step. These include: * State-of-the-art extraction techniques for organic and inorganic analytes * Sample preparation in biological measurements * Sample pretreatment in microscopy * Surface enhancement as a sample preparation tool in Raman and IR spectroscopy * Sample concentration and clean-up methods * Quality control steps Designed to serve as a text in an undergraduate or graduate level curriculum, Sample Preparation Techniques in Analytical Chemistry also provides an invaluable reference tool for analytical chemists in the chemical, biological, pharmaceutical, environmental, and materials sciences.
Categories: Science

Forensics and Clinical Applications of Solid Phase Extraction Second Edition

Forensics and Clinical Applications of Solid Phase Extraction  Second Edition

This volume explains the principles behind SPE and provides protocols to help readers master extraction problems.

Author: Thomas F. August

Publisher:

ISBN: 1315117398

Category: Electronic books

Page:

View: 561

"Solid Phase Extraction (SPE) has become a powerful and extensively used technique in the clean-up and concentration of samples in a wide variety of analytical techniques. This volume explains the principles behind SPE and provides protocols to help readers master extraction problems. These detailed methods are particularly suited to solving extraction problems in forensic, pharmaceutical, and clinical chemistry and include readily understandable explanations of the principals of pH, ion exchange, and co-polymeric mechanism-enhanced SPE. Each protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, a list of equipment and reagents, troubleshooting advice, and tips on how to avoid known pitfalls."--Provided by publisher.
Categories: Electronic books

Trace Environmental Quantitative Analysis

Trace Environmental Quantitative Analysis

This study offers insight into the principles of trace environmental quantitative analysis (TEQA), focusing on data reduction and interpretation, sample preparation and instrumental analysis from a wide range of matrices, including sludge, ...

Author: Paul R. Loconto

Publisher: CRC Press

ISBN: 0824745140

Category: Science

Page: 656

View: 805

This study offers insight into the principles of trace environmental quantitative analysis (TEQA), focusing on data reduction and interpretation, sample preparation and instrumental analysis from a wide range of matrices, including sludge, sediment, oil and air, as well as ground, waste and surface water. It draws on the author's own research with metal chelate solid-phase extraction.
Categories: Science

Solid Phase Extraction State of the Art and Future Perspectives

Solid Phase Extraction  State of the Art and Future Perspectives

Wells, M.J.M. Handling large volume samples: applications of SPE to environmental matrices. In Solid-Phase Extraction: Principles, Techniques, and Application, 1st ed.; Simpson, N.K.J., Ed.; CRC Press: Boca Raton, FL, USA, 2000. 3.

Author: Victoria Samanidou

Publisher: MDPI

ISBN: 9783039211586

Category: Science

Page: 176

View: 552

This book is a collection of 13 innovative papers describing the state of the art and the future perspectives in solid-phase extraction covering several analytical fields prior to the use of gas or liquid chromatographic analysis. New sorptive materials are presented including carbon nanohorn suprastructures on paper support, melamine sponge functionalized with urea–formaldehyde co-oligomers, chiral metal–organic frameworks, UiO-66-based metal–organic frameworks, and fabric phase sorptive media for various applications. Solid-phase extraction can be applied in several formats aside from the conventional cartridges or mini-column approach, e.g., online solid-phase extraction, dispersive solid-phase microextraction, and in-syringe micro-solid-phase extraction can be very helpful for analyte pre-concentration and sample clean-up. Polycyclic musks in aqueous samples, 8-Nitroguanine in DNA by chemical derivatization antibacterial diterpenes from the roots of salvia prattii, perfluoroalkyl substances (PFASs) in aater samples by bamboo charcoal-based SPE, parabens in environmental water samples, benzotriazoles as environmental pollutants, organochlorine pesticide residues in various fruit juices and water samples and synthetic peptide purification are among the applications cited in this collection. All these outstanding contributions highlight the necessity of this analytical step, present the advantages and disadvantages of each method and focus on the green analytical chemistry guidelines that have to be fulfilled in current analytical practices.
Categories: Science